{"id":69,"date":"2026-04-13T22:34:42","date_gmt":"2026-04-13T14:34:42","guid":{"rendered":"https:\/\/kongling.xin\/?p=69"},"modified":"2026-04-13T22:36:14","modified_gmt":"2026-04-13T14:36:14","slug":"%e5%88%9d%e6%ac%a1%e6%9c%89%e6%9c%ba%e5%90%88%e6%88%90%e5%ae%9e%e9%aa%8c%e6%93%8d%e4%bd%9c%e5%ad%a6%e4%b9%a0%e7%ac%94%e8%ae%b0","status":"publish","type":"post","link":"https:\/\/kongling.xin\/index.php\/2026\/04\/13\/%e5%88%9d%e6%ac%a1%e6%9c%89%e6%9c%ba%e5%90%88%e6%88%90%e5%ae%9e%e9%aa%8c%e6%93%8d%e4%bd%9c%e5%ad%a6%e4%b9%a0%e7%ac%94%e8%ae%b0\/","title":{"rendered":"\u521d\u6b21\u6709\u673a\u5408\u6210\u5b9e\u9a8c\u64cd\u4f5c\u5b66\u4e60\u7b14\u8bb0"},"content":{"rendered":"\n<p class=\"wp-block-paragraph\">\u672c\u6587\u7ae0\u6765\u81ea\u4e00\u4e2a\u521a\u521a\u52a0\u5165\u6709\u673a\u5316\u5b66\u9879\u76eesrp\u7684\u5c0f\u767b\uff0c\u76ee\u7684\u662f\u8bb0\u5f55\u4e00\u4e0b\u5b66\u4e60\u5230\u7684\u6709\u9650\u7684\u6709\u673a\u5316\u5b66\u5b9e\u9a8c\u64cd\u4f5c<\/p>\n\n\n\n<h2 class=\"wp-block-heading\">1. \u51c6\u5907\u5de5\u4f5c<\/h2>\n\n\n\n<p class=\"wp-block-paragraph\">\u6234PE\u624b\u5957\u3001\u4e01\u8148\u624b\u5957\u3001\u5b9e\u9a8c\u670d\u3001\u62a4\u76ee\u955c\u548c\u53e3\u7f69\uff0c\u505a\u597d\u4e2a\u4eba\u9632\u62a4\u3002<\/p>\n\n\n\n<h2 class=\"wp-block-heading\">2. \u53cd\u5e94\u88c5\u7f6e\u642d\u5efa<\/h2>\n\n\n\n<p class=\"wp-block-paragraph\">\u5728 Schlenk \u74f6\u4fa7\u652f\u7ba1\u65cb\u585e\u5904\u5747\u5300\u6d82\u62b9\u7845\u8102\uff0c\u8f6c\u52a8\u65cb\u585e\u4f7f\u5176\u5bc6\u5c01\u826f\u597d\u3002<\/p>\n\n\n\n<p class=\"wp-block-paragraph\">\u4f9d\u6b21\u5411\u74f6\u5185\u52a0\u5165\u78c1\u529b\u6405\u62cc\u5b50\u3001\u79f0\u91cf\u597d\u7684\u53cd\u5e94\u7269 A \u4e0e\u53cd\u5e94\u7269 B\uff0c\u518d\u52a0\u5165 20 mL \u65e0\u6c34 THF \u4f5c\u4e3a\u6eb6\u5242\u3002<\/p>\n\n\n\n<p class=\"wp-block-paragraph\">\u7528\u7ffb\u53e3\u6a61\u80f6\u585e\u5bc6\u5c01\u74f6\u53e3\uff0c\u901a\u8fc7 Schlenk \u7cfb\u7edf\u8fdb\u884c\u4e09\u6b21\u62bd\u771f\u7a7a \u2014 \u5145\u6c2e\u6c14\u64cd\u4f5c\uff0c\u6784\u5efa\u65e0\u6c34\u65e0\u6c27\u53cd\u5e94\u73af\u5883\u3002<\/p>\n\n\n\n<figure class=\"wp-block-image size-full\"><img loading=\"lazy\" decoding=\"async\" width=\"529\" height=\"289\" src=\"https:\/\/kongling.xin\/wp-content\/uploads\/2026\/04\/1776088101-44.webp\" alt=\"\" class=\"wp-image-76\" srcset=\"https:\/\/kongling.xin\/wp-content\/uploads\/2026\/04\/1776088101-44.webp 529w, https:\/\/kongling.xin\/wp-content\/uploads\/2026\/04\/1776088101-44-300x164.webp 300w\" sizes=\"auto, (max-width: 529px) 100vw, 529px\" \/><\/figure>\n\n\n\n<h2 class=\"wp-block-heading\">3. \u52a0\u5165\u8bd5\u5242<\/h2>\n\n\n\n<p class=\"wp-block-paragraph\"> \u5728\u53cd\u5e94\u74f6\u53e3\u5b89\u88c5\u6c2e\u6c14\u6c14\u7403\uff0c\u4f7f\u7528\u76ae\u7b4b\u548c\u80f6\u5e26\u56fa\u5b9a\u6c14\u7403\u4e0e\u6ce8\u5c04\u5668\uff0c\u7ef4\u6301\u4f53\u7cfb\u5fae\u6b63\u538b\u5e73\u8861\u6c14\u538b\u3002<\/p>\n\n\n\n<p class=\"wp-block-paragraph\">\u4fdd\u6301\u4fa7\u652f\u7ba1\u4e0e Schlenk \u7ba1\u7ebf\u8fde\u901a\uff0c\u5728\u60f0\u6027\u6c14\u6d41\u4fdd\u62a4\u4e0b\uff0c\u7528\u6ce8\u5c04\u5668\u5206\u522b\u7f13\u6162\u52a0\u5165\u918b\u9178\uff08AcOH\uff09\u548c\u4e19\u919b\u3002<\/p>\n\n\n\n<p class=\"wp-block-paragraph\">\u64cd\u4f5c\u65f6\u89c4\u8303\u4f7f\u7528\u6ce8\u5c04\u5668\uff0c\u907f\u514d\u9488\u5934\u671d\u5411\u81ea\u8eab\u53ca\u4ed6\u4eba\u3002<\/p>\n\n\n\n<p class=\"wp-block-paragraph\">\u6ce8\u610f\u6ce8\u5c04\u5668\u7528\u6cd5<\/p>\n\n\n\n<figure class=\"wp-block-image size-full is-resized\"><img loading=\"lazy\" decoding=\"async\" width=\"624\" height=\"198\" src=\"https:\/\/kongling.xin\/wp-content\/uploads\/2026\/04\/1776074810-11.png\" alt=\"\" class=\"wp-image-72\" style=\"aspect-ratio:3.151817049699989;width:481px;height:auto\" srcset=\"https:\/\/kongling.xin\/wp-content\/uploads\/2026\/04\/1776074810-11.png 624w, https:\/\/kongling.xin\/wp-content\/uploads\/2026\/04\/1776074810-11-300x95.png 300w\" sizes=\"auto, (max-width: 624px) 100vw, 624px\" \/><\/figure>\n\n\n\n<figure class=\"wp-block-image size-full is-resized\"><img loading=\"lazy\" decoding=\"async\" width=\"591\" height=\"426\" src=\"https:\/\/kongling.xin\/wp-content\/uploads\/2026\/04\/1776075149-22.png\" alt=\"\" class=\"wp-image-73\" style=\"width:479px;height:auto\" srcset=\"https:\/\/kongling.xin\/wp-content\/uploads\/2026\/04\/1776075149-22.png 591w, https:\/\/kongling.xin\/wp-content\/uploads\/2026\/04\/1776075149-22-300x216.png 300w\" sizes=\"auto, (max-width: 591px) 100vw, 591px\" \/><\/figure>\n\n\n\n<h2 class=\"wp-block-heading\">4. \u6405\u62cc\u4e0e\u53cd\u5e94<\/h2>\n\n\n\n<p class=\"wp-block-paragraph\">\u5f00\u542f\u78c1\u529b\u6405\u62cc\uff0c\u4f7f\u53cd\u5e94\u4f53\u7cfb\u6df7\u5408\u5747\u5300\uff0c\u5ba4\u6e29\uff08r.t.\uff09\u6761\u4ef6\u4e0b\u6405\u62cc\u8fc7\u591c\u53cd\u5e94\u3002<\/p>\n\n\n\n<h2 class=\"wp-block-heading\">5. \u8403\u53d6<\/h2>\n\n\n\n<p class=\"wp-block-paragraph\">\u5c06\u53cd\u5e94\u6db2\u8f6c\u79fb\u81f3\u5206\u6db2\u6f0f\u6597\uff0c\u7ecf\u9971\u548c\u98df\u76d0\u6c34\u6d17\u6da4\u540e\u8fdb\u884c\u6db2 - \u6db2\u8403\u53d6\uff0c\u9759\u7f6e\u5206\u5c42\u540e\u6536\u96c6\u4e0a\u5c42\u6709\u673a\u76f8\u3002<\/p>\n\n\n\n<figure class=\"wp-block-image size-full\"><img loading=\"lazy\" decoding=\"async\" width=\"534\" height=\"353\" src=\"https:\/\/kongling.xin\/wp-content\/uploads\/2026\/04\/1776089400-55.png\" alt=\"\" class=\"wp-image-77\" srcset=\"https:\/\/kongling.xin\/wp-content\/uploads\/2026\/04\/1776089400-55.png 534w, https:\/\/kongling.xin\/wp-content\/uploads\/2026\/04\/1776089400-55-300x198.png 300w\" sizes=\"auto, (max-width: 534px) 100vw, 534px\" \/><\/figure>\n\n\n\n<h2 class=\"wp-block-heading\">6. \u65cb\u84b8<\/h2>\n\n\n\n<p class=\"wp-block-paragraph\">\u91c7\u7528\u65cb\u8f6c\u84b8\u53d1\u5668\u9664\u53bb\u5927\u90e8\u5206\u6eb6\u5242\u3002\u64cd\u4f5c\u65f6\u6ce8\u610f\u89c2\u5bdf\u6c14\u6ce1\uff0c\u9632\u6b62\u66b4\u6cb8\u51b2\u6599\uff1b<\/p>\n\n\n\n<p class=\"wp-block-paragraph\">\u9075\u5faa\u5148\u62bd\u771f\u7a7a\u518d\u5347\u6e29\u3001\u7ed3\u675f\u540e\u5148\u653e\u7a7a\u518d\u5173\u95ed\u771f\u7a7a\u6cf5\u7684\u987a\u5e8f\u3002<\/p>\n\n\n\n<h2 class=\"wp-block-heading\">7. \u8584\u5c42\u8272\u8c31\uff08TLC\uff09\u5206\u6790<\/h2>\n\n\n\n<p class=\"wp-block-paragraph\">\u5c11\u91cf\u7c97\u4ea7\u7269\u8fdb\u884c TLC \u70b9\u677f\uff0c\u76d1\u6d4b\u53cd\u5e94\u8fdb\u7a0b\u4e0e\u4ea7\u7269\u7eaf\u5ea6\uff0c<\/p>\n\n\n\n<p class=\"wp-block-paragraph\">\u5e76\u4e3a\u540e\u7eed\u67f1\u5c42\u6790\u5206\u79bb\u7b5b\u9009\u5408\u9002\u7684\u6d17\u8131\u4f53\u7cfb\u3002<\/p>\n\n\n\n<h2 class=\"wp-block-heading\">8. \u67f1\u5c42\u6790\u5206\u79bb<\/h2>\n\n\n\n<p class=\"wp-block-paragraph\">\u5728\u5c42\u6790\u67f1\u5e95\u90e8\u586b\u5165\u9002\u91cf\u68c9\u82b1\uff0c\u4e8e\u901a\u98ce\u6a71\u5185\u901a\u8fc7\u52a0\u6599\u6f0f\u6597\u88c5\u586b\u7845\u80f6\u3002<\/p>\n\n\n\n<p class=\"wp-block-paragraph\">\u91c7\u7528\u6e7f\u6cd5\u4e0a\u6837\uff0c\u5728\u7845\u80f6\u4e0a\u5c42\u8986\u76d6\u4e00\u5c42\u77f3\u82f1\u7802\uff0c\u907f\u514d\u52a0\u5165\u6d17\u8131\u5242\u65f6\u51b2\u6563\u7845\u80f6\u8868\u9762\u3002<\/p>\n\n\n\n<p class=\"wp-block-paragraph\">\u4ee5\u4e8c\u6c2f\u7532\u70f7\uff08DCM\uff09\u4e0e\u4e59\u9178\u4e59\u916f\uff08EA\uff09\u6309\u4e0d\u540c\u6bd4\u4f8b\u914d\u5236\u68af\u5ea6\u6d17\u8131\u5242\uff0c\u52a0\u538b\u8fdb\u884c\u67f1\u5c42\u6790\u5206\u79bb\uff0c\u5206\u6bb5\u6536\u96c6\u6d17\u8131\u7ec4\u5206\u3002<\/p>\n\n\n\n<figure class=\"wp-block-image size-large is-resized\"><img loading=\"lazy\" decoding=\"async\" width=\"1024\" height=\"768\" src=\"https:\/\/kongling.xin\/wp-content\/uploads\/2026\/04\/1776089441-66-1024x768.jpg\" alt=\"\" class=\"wp-image-78\" style=\"aspect-ratio:1.3333416007341452;width:640px;height:auto\" srcset=\"https:\/\/kongling.xin\/wp-content\/uploads\/2026\/04\/1776089441-66-1024x768.jpg 1024w, https:\/\/kongling.xin\/wp-content\/uploads\/2026\/04\/1776089441-66-300x225.jpg 300w, https:\/\/kongling.xin\/wp-content\/uploads\/2026\/04\/1776089441-66-768x576.jpg 768w, https:\/\/kongling.xin\/wp-content\/uploads\/2026\/04\/1776089441-66-1536x1152.jpg 1536w, https:\/\/kongling.xin\/wp-content\/uploads\/2026\/04\/1776089441-66-2048x1536.jpg 2048w\" sizes=\"auto, (max-width: 1024px) 100vw, 1024px\" \/><\/figure>\n\n\n\n<h2 class=\"wp-block-heading\">9. \u65cb\u84b8\u540e\u5904\u7406<\/h2>\n\n\n\n<p class=\"wp-block-paragraph\">\u5c06\u6536\u96c6\u7684\u542b\u4ea7\u7269\u6d17\u8131\u6db2\u518d\u6b21\u4f7f\u7528\u65cb\u8f6c\u84b8\u53d1\u5668\u84b8\u9664\u5269\u4f59\u6eb6\u5242\uff0c\u6700\u7ec8\u5f97\u5230\u76ee\u6807\u4ea7\u7269\u3002<\/p>\n\n\n\n<p class=\"wp-block-paragraph\"><\/p>\n","protected":false},"excerpt":{"rendered":"<p>\u672c\u6587\u7ae0\u6765\u81ea\u4e00\u4e2a\u521a\u521a\u52a0\u5165\u6709\u673a\u5316\u5b66\u9879\u76eesrp\u7684\u5c0f\u767b\uff0c\u76ee\u7684\u662f\u8bb0\u5f55\u4e00\u4e0b\u5b66\u4e60\u5230\u7684\u6709\u9650\u7684\u6709\u673a\u5316\u5b66\u5b9e\u9a8c\u64cd\u4f5c 1. \u51c6\u5907\u5de5\u4f5c \u6234PE\u624b\u5957\u3001\u4e01\u8148\u624b\u5957 &#8230;<\/p>\n","protected":false},"author":1,"featured_media":78,"comment_status":"closed","ping_status":"closed","sticky":false,"template":"","format":"standard","meta":{"emotion":"","emotion_color":"","title_style":"","license":"","footnotes":""},"categories":[1],"tags":[],"class_list":["post-69","post","type-post","status-publish","format-standard","has-post-thumbnail","hentry","category-uncategorized"],"_links":{"self":[{"href":"https:\/\/kongling.xin\/index.php\/wp-json\/wp\/v2\/posts\/69","targetHints":{"allow":["GET"]}}],"collection":[{"href":"https:\/\/kongling.xin\/index.php\/wp-json\/wp\/v2\/posts"}],"about":[{"href":"https:\/\/kongling.xin\/index.php\/wp-json\/wp\/v2\/types\/post"}],"author":[{"embeddable":true,"href":"https:\/\/kongling.xin\/index.php\/wp-json\/wp\/v2\/users\/1"}],"replies":[{"embeddable":true,"href":"https:\/\/kongling.xin\/index.php\/wp-json\/wp\/v2\/comments?post=69"}],"version-history":[{"count":8,"href":"https:\/\/kongling.xin\/index.php\/wp-json\/wp\/v2\/posts\/69\/revisions"}],"predecessor-version":[{"id":104,"href":"https:\/\/kongling.xin\/index.php\/wp-json\/wp\/v2\/posts\/69\/revisions\/104"}],"wp:featuredmedia":[{"embeddable":true,"href":"https:\/\/kongling.xin\/index.php\/wp-json\/wp\/v2\/media\/78"}],"wp:attachment":[{"href":"https:\/\/kongling.xin\/index.php\/wp-json\/wp\/v2\/media?parent=69"}],"wp:term":[{"taxonomy":"category","embeddable":true,"href":"https:\/\/kongling.xin\/index.php\/wp-json\/wp\/v2\/categories?post=69"},{"taxonomy":"post_tag","embeddable":true,"href":"https:\/\/kongling.xin\/index.php\/wp-json\/wp\/v2\/tags?post=69"}],"curies":[{"name":"wp","href":"https:\/\/api.w.org\/{rel}","templated":true}]}}